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  1. University of Yangon

Effect of Sonication Time on the Production of Graphene by Electrochemical Exfoliation Method

http://hdl.handle.net/20.500.12678/0000002992
http://hdl.handle.net/20.500.12678/0000002992
bf107e4d-2e50-4d3d-8b3d-acdb79529fee
9682962e-a70f-437b-b5e6-a6eb7829d654
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DR DR AAT_Phys (2).pdf (714 Kb)
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Publication type
Journal article
Upload type
Publication
Title
Title Effect of Sonication Time on the Production of Graphene by Electrochemical Exfoliation Method
Language en
Authors
Htwe, Y.Z.N.
Mariatti, M.
Chow, W.S.
Y. Suda
Aye Aye Thant
Description
In this study, Graphene has been synthesized by using electrochemical exfoliation method. Effect of sonication times (15, 30 and 45 min) at room temperature on the production of graphene was investigated. The synthesized graphene were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR) and Atomic Force Microscopy (AFM). The crystal structure of the exfoliated graphene were analyzed using XRD. The graphene flakes exhibit a sharp peak centered at 26.5°corresponding to the (002) plane of graphene crystal. It is found that, the crystallite sizes is gradually decreased with increased in sonication time. The FTIR spectrum reveals the prominent appearance of C-O-H group which indicate that OH-radicals exist in conjunction with exfoliated graphene sheets. Graphene flakes with average thickness of 0.2 nm to 0.8nm wereobserved using AFM. The electrical conductivity results showed that 45 min sonication time produced the highestelectricalconductivity (1.38×102sm-1).
Keywords
electronchmical, Graphene
Identifier 10.1088/1742-6596/1082/1/012031
Conference papers
RCM&AMC
12–13 December 2017
Regional Conference on Materials and ASEAN Microscopy Conference 2017 (RCM & AMC 2017)
Penang, Malaysia
https://iopscience.iop.org/article
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